Pencampuran dengan Attritor Mill pada Sintesis Mg0,8Zn0,2TiO3

Sefrilita Risqi Adikaning Rani, S Suasmoro
Submission Date: 2016-07-25 10:18:19
Accepted Date: 2016-11-23 18:14:55

Abstract


Material Mg0.8Zn0,2TiO3 disintesis menggunakan metode pencampuran attritor dengan variasi waktu milling 2 jam, 4 jam dan 6 jam. Hasil pencampuran dengan attritor menghasilkan  distribusi ukuran serbuk dalam orde submikronik. Keseragaman distribusi ukuran serbuk yang tinggi diperoleh dari serbuk hasil milling selama 6 jam yaitu sebesar 351,6 nm. Kalsinasi pada termperatur 950oC untuk serbuk campuran yang dimilling 6 jam memperlihatkan terbentuknya fasa tunggal dari (Mg/Zn)TiO3. Analisa dilakukan dengan menggunakan software match2.


Keywords


Attritor;(Mg/Zn)TiO3;milling

References


M. Saukani and S. Suasmoro, “Characterization of Mg0. 8Zn0. 2TiO3 Prepared via Liquid Phase Sintering,” in Advanced Materials Research, 2015, vol. 1112, pp. 11–14.

M. Zhang, L. Li, W. Xia, and Q. Liao, “Structure and properties analysis for MgTiO3 and (Mg0.97M0.03)TiO3 (M = Ni, Zn, Co and Mn) microwave dielectric materials,” J. Alloys Compd., vol. 537, pp. 76–79, Oct. 2012.

H. J. Jo, J. S. Kim, and E. S. Kim, “Microwave dielectric properties of MgTiO3-based ceramics,” Ceram. Int., vol. 41, Supplement 1, pp. S530–S536, Jul. 2015.

A. Ullah, Y. Iqbal, T. Mahmood, A. Mahmood, A. Naeem, and M. Hamayun, “Kinetic analysis on the synthesis of Mg0.95Zn0.05TiO3 microwave dielectric ceramic by polymeric precursor method,” Ceram. Int., vol. 41, no. 10, Part B, pp. 15089–15096, Dec. 2015.

H. T. Wu, Y. S. Jiang, Y. J. Cui, X. H. Zhang, X. Jia, and Y. L. Yue, “Improvements in the Sintering Behavior and Microwave Dielectric Properties of Geikielite-Type MgTiO3 Ceramics,” J. Electron. Mater., vol. 42, no. 3, pp. 445–451, Dec. 2012.

K. P. Surendran, A. Wu, P. M. Vilarinho, and V. M. Ferreira, “Sol−Gel Synthesis of Low-Loss MgTiO3 Thin Films by a Non-Methoxyethanol Route,” Chem. Mater., vol. 20, no. 13, pp. 4260–4267, Jul. 2008.

H. Cheng, B. Xu, and J. Ma, “Preparation of MgTiO3 by an improved chemical co-precipitation method,” J. Mater. Sci. Lett., vol. 16, no. 19, pp. 1570–1572, Oct. 1997.

G. Parthasarathy and S. V. Manorama, “A novel method for synthesizing nano-crystalline MgTiO3 geikielite,” Bull. Mater. Sci., vol. 30, no. 1, pp. 19–21, Feb. 2008.

G. Pfaff, “Peroxide route for synthesis of magnesium titanate powders of various compositions,” Ceram. Int., vol. 20, no. 2, pp. 111–116, Jan. 1994.

X. Zhou, Y. Yuan, L. Xiang, and Y. Huang, “Synthesis of MgTiO3 by solid state reaction and characteristics with addition,” J. Mater. Sci., vol. 42, no. 16, pp. 6628–6632, May 2007.

J. B. Huang, B. Yang, C. Y. Yu, G. F. Zhang, H. Xue, Z. X. Xiong, G. Viola, R. Donnan, H. X. Yan, and M. J. Reece, “Microwave and terahertz dielectric properties of MgTiO3–CaTiO3 ceramics,” Mater. Lett., vol. 138, pp. 225–227, Jan. 2015.

F. U. Ermawati, S. Pratapa, S. Suasmoro, T. Hübert, and U. Banach, “Preparation and structural study of Mg1−x Zn x TiO3 ceramics and their dielectric properties from 1 Hz to 7.7 GHz,” J. Mater. Sci. Mater. Electron., vol. 27, no. 7, pp. 6637–6645, Mar. 2016.

R. Angela and S. Pratapa, “Sintesis MgTiO3 dengan Variasi Temperatur Kalsinasi Menggunakan Metode Pencampuran Larutan,” J. Sains Dan Seni ITS, vol. 1, no. 1, pp. B73–B75, 2012.

K. A. Gavhane, Unit Operations-i Fluid Flow and Mechanical Operations. Nirali Prakashan, 2009.

R. A. Varin, T. Czujko, and Z. S. Wronski, Nanomaterials for Solid State Hydrogen Storage. Springer Science & Business Media, 2009.


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